Sharp, vertical-walled tips for SFM imaging of steep or soft samples

Keller, D. ; Deputy, D. ; Alduino, A. ; Luo, K.

Amsterdam : Elsevier
ISSN:
0304-3991
Source:
Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
Topics:
Electrical Engineering, Measurement and Control Technology
Natural Sciences in General
Physics
Type of Medium:
Electronic Resource
URL:
_version_ 1798291809680490496
autor Keller, D.
Deputy, D.
Alduino, A.
Luo, K.
autorsonst Keller, D.
Deputy, D.
Alduino, A.
Luo, K.
book_url http://linkinghub.elsevier.com/retrieve/pii/0304-3991(92)90470-5
datenlieferant nat_lic_papers
fussnote For samples with steep-walled features, for example semiconductors devices and mammalian cells, the STM or SFM will produce faithful images only if the probe tip is very sharp, that is, if the end radius of curvature and the opening angle are small. Sharp tips are also less strongly attracted to the sample surface by van der Waals interactions, and so can be operated at smaller net force. This is important for soft samples or samples that are not well anchored to the substrate, i.e., biological molecules. Two methods are described by which essentially cylindrical, vertical-walled tips can be made. In the first method a long thin ''flagpole'' is carved from a tungsten STM tip by a beam of focused gallium ions. In the second method a focused electron beam is used to deposit tall thin spikes of hard carbon on commercial silicon-nitride SFM cantilevers. SFM images of steep-walled grating structures made using e-beam tips show the correct dimensions and sidewall angles, in sharp contrast to the distorted images that result when standard commercial tips are used. The e-beam method can also be used to create hooked tips with well-defined geometry for imaging undercut structures.
hauptsatz hsatz_simple
identnr NLZ178327522
issn 0304-3991
journal_name Ultramicroscopy
materialart 1
package_name Elsevier
publikationsort Amsterdam
publisher Elsevier
reference 42-44 (1992), S. 1481-1489
search_space articles
shingle_author_1 Keller, D.
Deputy, D.
Alduino, A.
Luo, K.
shingle_author_2 Keller, D.
Deputy, D.
Alduino, A.
Luo, K.
shingle_author_3 Keller, D.
Deputy, D.
Alduino, A.
Luo, K.
shingle_author_4 Keller, D.
Deputy, D.
Alduino, A.
Luo, K.
shingle_catch_all_1 Keller, D.
Deputy, D.
Alduino, A.
Luo, K.
Sharp, vertical-walled tips for SFM imaging of steep or soft samples
0304-3991
03043991
Elsevier
shingle_catch_all_2 Keller, D.
Deputy, D.
Alduino, A.
Luo, K.
Sharp, vertical-walled tips for SFM imaging of steep or soft samples
0304-3991
03043991
Elsevier
shingle_catch_all_3 Keller, D.
Deputy, D.
Alduino, A.
Luo, K.
Sharp, vertical-walled tips for SFM imaging of steep or soft samples
0304-3991
03043991
Elsevier
shingle_catch_all_4 Keller, D.
Deputy, D.
Alduino, A.
Luo, K.
Sharp, vertical-walled tips for SFM imaging of steep or soft samples
0304-3991
03043991
Elsevier
shingle_title_1 Sharp, vertical-walled tips for SFM imaging of steep or soft samples
shingle_title_2 Sharp, vertical-walled tips for SFM imaging of steep or soft samples
shingle_title_3 Sharp, vertical-walled tips for SFM imaging of steep or soft samples
shingle_title_4 Sharp, vertical-walled tips for SFM imaging of steep or soft samples
sigel_instance_filter dkfz
geomar
wilbert
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source_archive Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
timestamp 2024-05-06T08:38:31.526Z
titel Sharp, vertical-walled tips for SFM imaging of steep or soft samples
titel_suche Sharp, vertical-walled tips for SFM imaging of steep or soft samples
For samples with steep-walled features, for example semiconductors devices and mammalian cells, the STM or SFM will produce faithful images only if the probe tip is very sharp, that is, if the end radius of curvature and the opening angle are small. Sharp tips are also less strongly attracted to the sample surface by van der Waals interactions, and so can be operated at smaller net force. This is important for soft samples or samples that are not well anchored to the substrate, i.e., biological molecules. Two methods are described by which essentially cylindrical, vertical-walled tips can be made. In the first method a long thin ''flagpole'' is carved from a tungsten STM tip by a beam of focused gallium ions. In the second method a focused electron beam is used to deposit tall thin spikes of hard carbon on commercial silicon-nitride SFM cantilevers. SFM images of steep-walled grating structures made using e-beam tips show the correct dimensions and sidewall angles, in sharp contrast to the distorted images that result when standard commercial tips are used. The e-beam method can also be used to create hooked tips with well-defined geometry for imaging undercut structures.
topic ZN
TA-TD
U
uid nat_lic_papers_NLZ178327522