Thione complexes of group IIB dihalides. X-ray crystal structure of Cd(ETTC)"2I"2

ISSN:
0277-5387
Source:
Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
Topics:
Chemistry and Pharmacology
Type of Medium:
Electronic Resource
URL:
http://linkinghub.elsevier.com/retrieve/pii/S0277-5387(00)83865-6
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autor Castineiras, A.
Vidal, C.F.
Bastida, R.
Macias, A.
Hiller, W.
autorsonst Castineiras, A.
Vidal, C.F.
Bastida, R.
Macias, A.
Hiller, W.
book_url http://linkinghub.elsevier.com/retrieve/pii/S0277-5387(00)83865-6
datenlieferant nat_lic_papers
fussnote Complexes having the empirical formulae M(ETTC)"2X"2 (M = Zn or Hg, X = Br or I, ETTC = ethylene trithiocarbonate), Cd(ETTC)"2I"2 and Hg(ETTC)X"2 (X = Cl, Br or I) were obtained by the reaction of zinc, cadmium or mercury dihalides in dichloromethane or ethanol with ETTC. The structures of the compounds were characterized by ^1H NMR and IR spectrometry, conductance measurements and elemental analysis. The X-ray crystal structure of Cd(ETTC)"2I"2 has been determined using counter data and refined to an R value of 0.045. The unit cell constants are a = 1586.3(2), b = 699.7(1) and c = 724.9(3) pm, the space group is Pmn2"1 and Z = 2. Coordination about the cadmium atom is tetrahedral.
hauptsatz hsatz_simple
identnr NLZ175218927
issn 0277-5387
journal_name Polyhedron
materialart 1
package_name Elsevier
publikationsort Amsterdam
publisher Elsevier
reference 7 (1988), S. 2503-2508
search_space articles
shingle_author_1 Castineiras, A.
Vidal, C.F.
Bastida, R.
Macias, A.
Hiller, W.
shingle_author_2 Castineiras, A.
Vidal, C.F.
Bastida, R.
Macias, A.
Hiller, W.
shingle_author_3 Castineiras, A.
Vidal, C.F.
Bastida, R.
Macias, A.
Hiller, W.
shingle_author_4 Castineiras, A.
Vidal, C.F.
Bastida, R.
Macias, A.
Hiller, W.
shingle_catch_all_1 Castineiras, A.
Vidal, C.F.
Bastida, R.
Macias, A.
Hiller, W.
Thione complexes of group IIB dihalides. X-ray crystal structure of Cd(ETTC)"2I"2
0277-5387
02775387
Elsevier
shingle_catch_all_2 Castineiras, A.
Vidal, C.F.
Bastida, R.
Macias, A.
Hiller, W.
Thione complexes of group IIB dihalides. X-ray crystal structure of Cd(ETTC)"2I"2
0277-5387
02775387
Elsevier
shingle_catch_all_3 Castineiras, A.
Vidal, C.F.
Bastida, R.
Macias, A.
Hiller, W.
Thione complexes of group IIB dihalides. X-ray crystal structure of Cd(ETTC)"2I"2
0277-5387
02775387
Elsevier
shingle_catch_all_4 Castineiras, A.
Vidal, C.F.
Bastida, R.
Macias, A.
Hiller, W.
Thione complexes of group IIB dihalides. X-ray crystal structure of Cd(ETTC)"2I"2
0277-5387
02775387
Elsevier
shingle_title_1 Thione complexes of group IIB dihalides. X-ray crystal structure of Cd(ETTC)"2I"2
shingle_title_2 Thione complexes of group IIB dihalides. X-ray crystal structure of Cd(ETTC)"2I"2
shingle_title_3 Thione complexes of group IIB dihalides. X-ray crystal structure of Cd(ETTC)"2I"2
shingle_title_4 Thione complexes of group IIB dihalides. X-ray crystal structure of Cd(ETTC)"2I"2
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source_archive Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
timestamp 2024-05-06T08:37:38.012Z
titel Thione complexes of group IIB dihalides. X-ray crystal structure of Cd(ETTC)"2I"2
titel_suche Thione complexes of group IIB dihalides. X-ray crystal structure of Cd(ETTC)"2I"2
Complexes having the empirical formulae M(ETTC)"2X"2 (M = Zn or Hg, X = Br or I, ETTC = ethylene trithiocarbonate), Cd(ETTC)"2I"2 and Hg(ETTC)X"2 (X = Cl, Br or I) were obtained by the reaction of zinc, cadmium or mercury dihalides in dichloromethane or ethanol with ETTC. The structures of the compounds were characterized by ^1H NMR and IR spectrometry, conductance measurements and elemental analysis. The X-ray crystal structure of Cd(ETTC)"2I"2 has been determined using counter data and refined to an R value of 0.045. The unit cell constants are a = 1586.3(2), b = 699.7(1) and c = 724.9(3) pm, the space group is Pmn2"1 and Z = 2. Coordination about the cadmium atom is tetrahedral.
topic V
uid nat_lic_papers_NLZ175218927