Synthesis and characterization of Nano NiCo 2 O 4 by microwave promoted precipitation method
| Publication Date: |
2018-09-01
|
|---|---|
| Publisher: |
Institute of Physics (IOP)
|
| Print ISSN: |
1757-8981
|
| Electronic ISSN: |
1757-899X
|
| Topics: |
Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
|
| Published by: |
| _version_ | 1839208172551667712 |
|---|---|
| autor | M Yang, A Chen, Y Zhang and L Le |
| beschreibung | Nanostructured spinel NiCo 2 O 4 was synthesized via a facile and effective microwave promoted precipitation method with a simple post-calcination treatment. The crystalline and textural structure and morphology of the samples were characterized by X-ray diffraction, field-emission scanning electron microscopy, and Brunauer-Emmett-Teller techniques. The influence of several parameters on the morphology of NiCo 2 O 4 , such as Ni/Co mole ratio, amount of precipitation agent urea, amount of ethylene glycol (EG), were investigated, and the optimal reaction conditions (Ni/Co = 1.0:2.5, urea 0.30 g, and EG 30 ml) were obtained. Under the optimal reaction conditions, the prepared spinel NiCo 2 O 4 has a regular porous nanosheet structure. The nanosheet spinel NiCo 2 O 4 possesses a high surface area of 124.8 m 2 /g, a narrow pore size distribution of 3–10 nm, and a mean pore diameter of 5.4 nm. |
| citation_standardnr | 6326706 |
| datenlieferant | ipn_articles |
| feed_id | 123476 |
| feed_publisher | Institute of Physics (IOP) |
| feed_publisher_url | http://www.iop.org/ |
| insertion_date | 2018-09-01 |
| journaleissn | 1757-899X |
| journalissn | 1757-8981 |
| publikationsjahr_anzeige | 2018 |
| publikationsjahr_facette | 2018 |
| publikationsjahr_intervall | 7984:2015-2019 |
| publikationsjahr_sort | 2018 |
| publisher | Institute of Physics (IOP) |
| quelle | IOP Conference Series: Materials Science and Engineering |
| relation | http://iopscience.iop.org/1757-899X/397/1/012087 |
| search_space | articles |
| shingle_author_1 | M Yang, A Chen, Y Zhang and L Le |
| shingle_author_2 | M Yang, A Chen, Y Zhang and L Le |
| shingle_author_3 | M Yang, A Chen, Y Zhang and L Le |
| shingle_author_4 | M Yang, A Chen, Y Zhang and L Le |
| shingle_catch_all_1 | Synthesis and characterization of Nano NiCo 2 O 4 by microwave promoted precipitation method Nanostructured spinel NiCo 2 O 4 was synthesized via a facile and effective microwave promoted precipitation method with a simple post-calcination treatment. The crystalline and textural structure and morphology of the samples were characterized by X-ray diffraction, field-emission scanning electron microscopy, and Brunauer-Emmett-Teller techniques. The influence of several parameters on the morphology of NiCo 2 O 4 , such as Ni/Co mole ratio, amount of precipitation agent urea, amount of ethylene glycol (EG), were investigated, and the optimal reaction conditions (Ni/Co = 1.0:2.5, urea 0.30 g, and EG 30 ml) were obtained. Under the optimal reaction conditions, the prepared spinel NiCo 2 O 4 has a regular porous nanosheet structure. The nanosheet spinel NiCo 2 O 4 possesses a high surface area of 124.8 m 2 /g, a narrow pore size distribution of 3–10 nm, and a mean pore diameter of 5.4 nm. M Yang, A Chen, Y Zhang and L Le Institute of Physics (IOP) 1757-8981 17578981 1757-899X 1757899X |
| shingle_catch_all_2 | Synthesis and characterization of Nano NiCo 2 O 4 by microwave promoted precipitation method Nanostructured spinel NiCo 2 O 4 was synthesized via a facile and effective microwave promoted precipitation method with a simple post-calcination treatment. The crystalline and textural structure and morphology of the samples were characterized by X-ray diffraction, field-emission scanning electron microscopy, and Brunauer-Emmett-Teller techniques. The influence of several parameters on the morphology of NiCo 2 O 4 , such as Ni/Co mole ratio, amount of precipitation agent urea, amount of ethylene glycol (EG), were investigated, and the optimal reaction conditions (Ni/Co = 1.0:2.5, urea 0.30 g, and EG 30 ml) were obtained. Under the optimal reaction conditions, the prepared spinel NiCo 2 O 4 has a regular porous nanosheet structure. The nanosheet spinel NiCo 2 O 4 possesses a high surface area of 124.8 m 2 /g, a narrow pore size distribution of 3–10 nm, and a mean pore diameter of 5.4 nm. M Yang, A Chen, Y Zhang and L Le Institute of Physics (IOP) 1757-8981 17578981 1757-899X 1757899X |
| shingle_catch_all_3 | Synthesis and characterization of Nano NiCo 2 O 4 by microwave promoted precipitation method Nanostructured spinel NiCo 2 O 4 was synthesized via a facile and effective microwave promoted precipitation method with a simple post-calcination treatment. The crystalline and textural structure and morphology of the samples were characterized by X-ray diffraction, field-emission scanning electron microscopy, and Brunauer-Emmett-Teller techniques. The influence of several parameters on the morphology of NiCo 2 O 4 , such as Ni/Co mole ratio, amount of precipitation agent urea, amount of ethylene glycol (EG), were investigated, and the optimal reaction conditions (Ni/Co = 1.0:2.5, urea 0.30 g, and EG 30 ml) were obtained. Under the optimal reaction conditions, the prepared spinel NiCo 2 O 4 has a regular porous nanosheet structure. The nanosheet spinel NiCo 2 O 4 possesses a high surface area of 124.8 m 2 /g, a narrow pore size distribution of 3–10 nm, and a mean pore diameter of 5.4 nm. M Yang, A Chen, Y Zhang and L Le Institute of Physics (IOP) 1757-8981 17578981 1757-899X 1757899X |
| shingle_catch_all_4 | Synthesis and characterization of Nano NiCo 2 O 4 by microwave promoted precipitation method Nanostructured spinel NiCo 2 O 4 was synthesized via a facile and effective microwave promoted precipitation method with a simple post-calcination treatment. The crystalline and textural structure and morphology of the samples were characterized by X-ray diffraction, field-emission scanning electron microscopy, and Brunauer-Emmett-Teller techniques. The influence of several parameters on the morphology of NiCo 2 O 4 , such as Ni/Co mole ratio, amount of precipitation agent urea, amount of ethylene glycol (EG), were investigated, and the optimal reaction conditions (Ni/Co = 1.0:2.5, urea 0.30 g, and EG 30 ml) were obtained. Under the optimal reaction conditions, the prepared spinel NiCo 2 O 4 has a regular porous nanosheet structure. The nanosheet spinel NiCo 2 O 4 possesses a high surface area of 124.8 m 2 /g, a narrow pore size distribution of 3–10 nm, and a mean pore diameter of 5.4 nm. M Yang, A Chen, Y Zhang and L Le Institute of Physics (IOP) 1757-8981 17578981 1757-899X 1757899X |
| shingle_title_1 | Synthesis and characterization of Nano NiCo 2 O 4 by microwave promoted precipitation method |
| shingle_title_2 | Synthesis and characterization of Nano NiCo 2 O 4 by microwave promoted precipitation method |
| shingle_title_3 | Synthesis and characterization of Nano NiCo 2 O 4 by microwave promoted precipitation method |
| shingle_title_4 | Synthesis and characterization of Nano NiCo 2 O 4 by microwave promoted precipitation method |
| timestamp | 2025-07-31T23:46:36.677Z |
| titel | Synthesis and characterization of Nano NiCo 2 O 4 by microwave promoted precipitation method |
| titel_suche | Synthesis and characterization of Nano NiCo 2 O 4 by microwave promoted precipitation method |
| topic | ZL |
| uid | ipn_articles_6326706 |